methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate

Base Information

Chemical Name:methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate
CAS No.:1210758-27-2
Molecular Formula:C₁₅H₁₆N₄O₆
Molecular Weight:348.315
Hs Code.:

Synonyms:methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate

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Chemical Property of methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate

Chemical Property:

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Technology Process of methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate

There total 3 articles about methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.6%

: 6306-52-1
L-valine methylester hydrochloride

: 96898-36-1
ethyl 3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxylate

: 1210758-27-2
methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate

Guidance literature:: With triethylamine; In ethanol; Reflux;

Reference yield:

: 619-72-7
4-nitrobenzonitrile

: 1210758-27-2
methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; potassium carbonate / ethanol / 5 h / 80 °C

2: pyridine / chloroform / 14.75 h / 0 - 60 °C

3: triethylamine / ethanol / 16 h / 80 °C

With pyridine; hydroxylamine hydrochloride; potassium carbonate; triethylamine; In ethanol; chloroform;
DOI:10.1016/j.ejmech.2012.05.016

Reference yield:

: 192332-48-2
N'-hydroxy-4-nitrobenzimidamide

: 1210758-27-2
methyl 2-(3-(4-nitrophenyl)-1,2,4-oxadiazole-5-carboxamido)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / chloroform / 14.75 h / 0 - 60 °C

2: triethylamine / ethanol / 16 h / 80 °C

With pyridine; triethylamine; In ethanol; chloroform;
DOI:10.1016/j.ejmech.2012.05.016