3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol

Base Information

Chemical Name:3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol
CAS No.:1448816-25-8
Molecular Formula:C₁₇H₁₈N₄O₆
Molecular Weight:374.353
Hs Code.:

Synonyms:3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol

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Chemical Property of 3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol

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Technology Process of 3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol

There total 8 articles about 3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1448816-39-4
5-(2,3-bis(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

: 1448816-25-8
3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 7h; under 3102.97 Torr;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 189700-10-5
2,3-bis(benzyloxy)-4-methoxybenzaldehyde

: 1448816-25-8
3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol

Guidance literature:: Multi-step reaction with 6 steps

1: sodium dihydrogenphosphate; sodium perchlorate / dihydrogen peroxide / 6 h / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

4: oxalyl dichloride; pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

5: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

6: palladium 10% on activated carbon; hydrogen / methanol / 7 h / 3102.97 Torr

With pyridine; sodium dihydrogenphosphate; sodium azide; oxalyl dichloride; palladium 10% on activated carbon; sodium perchlorate; hydrogen; triethylamine; N,N-dimethyl-formamide; In methanol; dichloromethane; dihydrogen peroxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 1448816-34-9
2,3-bis(benzyloxy)-4-methoxy-N-(3,4,5-trimethoxyphenyl)benzamide

: 1448816-25-8
3-methoxy-6-(1-(3,4,5-trimethoxyphenyl)-1H-tetrazol-5-yl)benzene-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 7 h / 3102.97 Torr

With pyridine; sodium azide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004