2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol

Base Information

Chemical Name:2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol
CAS No.:62744-17-6
Molecular Formula:C₃₂H₃₁NO₄
Molecular Weight:493.602
Hs Code.:

2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6<i>H</i>-isoquino[3,2-<i>a</i>]isoquinolin-11-ol

Synonyms:2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol

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Chemical Property of 2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol

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Technology Process of 2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol

There total 1 articles about 2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62744-17-6
2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol

Guidance literature:: Tetrahydroisochinolin 15b, HCHO (Schema I);
DOI:10.1021/jo00439a017

Reference yield:

: 62744-17-6
2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol

: 32634-68-7
(2S,3S)-di-4-toluoyltartaric acid

: 1422185-91-8
C₃₂H₃₁NO₄*C₂₀H₁₈O₈

Guidance literature:: 2,10-bis-benzyloxy-3-methoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-ol; With Di-p-toluoyl-L-tartaric acid; In ethyl acetate; for 4h; Reflux;

With ammonium hydroxide; In water; ethyl acetate;

(2S,3S)-di-4-toluoyltartaric acid; In ethyl acetate; for 4h; Reflux;