(S)-N₁,N₁,N₂,N₂-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine

Base Information

• Chemical Name: (S)-N₁,N₁,N₂,N₂-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine
• CAS No.: 1366421-73-9
• Molecular Formula: C₃₅H₅₃N₃
• Molecular Weight: 515.826

Synonyms:(S)-N₁,N₁,N₂,N₂-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine

Chemical Property of (S)-N₁,N₁,N₂,N₂-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine

Chemical Property:

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Technology Process of (S)-N₁,N₁,N₂,N₂-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine

There total 4 articles about (S)-N₁,N₁,N₂,N₂-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(S)-N1,N1,N2,N2-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine hydrochloride (1366421-71-7) → (S)-N1,N1,N2,N2-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine (1366421-73-9)

Guidance literature:

With sodium hydroxide; In dichloromethane; Inert atmosphere;

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + N-cyclohexyl-cyclohexanamine (101-83-7) → (S)-N1,N1,N2,N2-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine (1366421-73-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: dichloromethane / 4 h / 20 °C

1.2: 10 h / 20 °C

2.1: sodium hydroxide / dichloromethane

With sodium hydroxide; In dichloromethane;

DOI:10.1021/ja3015764

Reference yield:

1-chloro-2,3-bis(dicyclohexylamino)cyclopropenium chloride + rac-methylbenzylamine (618-36-0) → (S)-N1,N1,N2,N2-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine (1366421-73-9)

Guidance literature:

1-chloro-2,3-bis(dicyclohexylamino)cyclopropenium chloride; rac-methylbenzylamine;

With sodium hydroxide; In dichloromethane;

DOI:10.1039/c4sc02402h

upstream raw materials:

(S)-N₁,N₁,N₂,N₂-tetracyclohexyl-3-(1-phenylethylimino)cycloprop-1-ene-1,2-diamine hydrochloride

(S)-1-phenyl-ethylamine

N-cyclohexyl-cyclohexanamine

rac-methylbenzylamine

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