4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate

Base Information

Chemical Name:4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate
CAS No.:252868-90-9
Molecular Formula:C₅₄H₉₃O₁₁PS
Molecular Weight:981.366
Hs Code.:

Synonyms:4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate

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Chemical Property of 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate

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Technology Process of 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate

There total 3 articles about 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)H-phosphonate

: 252868-90-9
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate

Guidance literature:: With pyridine; sulfur; In toluene; at 20 ℃; for 8h;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 147632-69-7
triethylammonium 1,2-di-O-hexadecanoyl-sn-glycerol 3-hydrogenphosphonate

: 252868-90-9
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate

Guidance literature:: Multi-step reaction with 2 steps

1: 5,5-dimethyl-2-oxo-2-chloro-1,3,2-dioxaphosphorinane; Py / 1 h / 20 °C

2: 47 percent / sulfur; Py / toluene / 8 h / 20 °C

With pyridine; 2-chloro-5,5-dimethyl[1,3,2]dioxaphosphinane 2-oxide; sulfur; In toluene; 1: Substitution / 2: Oxidation;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 156593-40-7
D-4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-myo-inositol

: 252868-90-9
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphorothioate

Guidance literature:: Multi-step reaction with 2 steps

1: 5,5-dimethyl-2-oxo-2-chloro-1,3,2-dioxaphosphorinane; Py / 1 h / 20 °C

2: 47 percent / sulfur; Py / toluene / 8 h / 20 °C

With pyridine; 2-chloro-5,5-dimethyl[1,3,2]dioxaphosphinane 2-oxide; sulfur; In toluene; 1: Substitution / 2: Oxidation;
DOI:10.1016/S0040-4020(99)00793-0