di-O-methyl-(3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

Base Information

Chemical Name:di-O-methyl-(3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate
CAS No.:646536-79-0
Molecular Formula:C₃₅H₄₂O₄SiSn
Molecular Weight:673.512
Hs Code.:

Synonyms:di-O-methyl-(3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

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Chemical Property of di-O-methyl-(3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

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Technology Process of di-O-methyl-(3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

There total 1 articles about di-O-methyl-(3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 63104-44-9
dimethyl 2,2-di(prop-2-ynyl)malonate

: 185962-47-4
tert-butyldimethylsilyl triphenylstannane

: 646536-79-0
di-O-methyl-(3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In benzene; stirring of soln. of di-O-methyldipropargylmalonate, (tert-butyldimethylsilyl)-triphenylstannane, Pd2(dba)3 and tris-(pentafluorophenyl)phosphine in benzene at room temp. for 16 h (J. Am. Chem. Soc. 2000, 122, 8579); evapn. of solvent, chromy. on silica gel (hexane/diethyl ether: 95:5; 80:20);
DOI:10.1021/ja035136m