(S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde

Base Information

• Chemical Name: (S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde
• CAS No.: 215609-87-3
• Molecular Formula: C₂₃H₂₇NO₅S
• Molecular Weight: 429.537

Synonyms:(S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde

Chemical Property of (S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde

Chemical Property:

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Technology Process of (S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde

There total 1 articles about (S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-(3,4-dimethoxyphenyl)-3-[(N-p-tolylsulfonyl)-2,2-diethoxyethylamino]-1-cyclohexene (244250-95-1) → (S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde (215609-87-3)

Guidance literature:

With silica gel; iron(III) chloride; In acetone; at 20 ℃; for 0.666667h;

DOI:10.1021/jo030309b

Reference yield: 89.0%

(S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde (215609-87-3) → (1S,2R,6S,7R)-6-(3,4-Dimethoxy-phenyl)-8-(toluene-4-sulfonyl)-10-oxa-8-aza-tricyclo[5.2.1.02,6]decane

Guidance literature:

With tin(IV) chloride; Ambient temperature;

DOI:10.1021/jo9815249

Reference yield: 60.0%

(S)-N-[2-(3,4-dimethoxyphenyl)cyclohex-1-enyl]-N-p-tolylsulfonyl-2-aminoacetaldehyde (215609-87-3) → (3R,3aS,7aS)-N-p-tolylsulfonyl-3-hydroxy-3a-(3,4-dimethoxyphenyl)-2,3,3a,6,7,7a-hexahydroindole

Guidance literature:

With 4 A molecular sieve; In toluene; at 230 - 240 ℃; for 1.33333h;

DOI:10.1021/jo030309b

upstream raw materials:

(S)-2-(3,4-dimethoxyphenyl)-3-[(N-p-tolylsulfonyl)-2,2-diethoxyethylamino]-1-cyclohexene

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