(2R,2′S,R_S)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine

Base Information

• Chemical Name: (2R,2′S,R_S)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine
• CAS No.: 1597449-86-9
• Molecular Formula: C₂₄H₃₈N₂O₃S
• Molecular Weight: 434.643

Synonyms:(2R,2′S,R_S)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine

Chemical Property of (2R,2′S,R_S)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine

Chemical Property:

Purity/Quality:

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Technology Process of (2R,2′S,R_S)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine

There total 1 articles about (2R,2′S,R_S)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

cis-3-hexene (7642-09-3) + (2R,2′S,RS)-1-(benzyloxycarbonyl)-2-[2′-tert-(butylsulfinamide)-4′-pentenyl]piperidine (1407484-43-8) → (2R,2′S,RS)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine (1597449-86-9)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; In dichloromethane; at 40 ℃; for 6h; Schlenk technique; Inert atmosphere;

DOI:10.1021/jo500446f

Reference yield:

(2R,2′S,RS)-(N-benzyloxycarbonyl)-2-[(2′-tert-butylsulfinamide)-4′-heptenyl]piperidine (1597449-86-9) → C20H30N2O2

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 23 ℃; for 1h; Inert atmosphere;

DOI:10.1021/jo500446f

upstream raw materials:

cis-3-hexene

(2R,2′S,R_S)-1-(benzyloxycarbonyl)-2-[2′-tert-(butylsulfinamide)-4′-pentenyl]piperidine

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