Technology Process of C20H15N3O
There total 2 articles about C20H15N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; potassium carbonate;
In
water; dimethyl sulfoxide;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2012.10.048
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 7 h / 100 °C / Inert atmosphere
2: tricyclohexylphosphine tetrafluoroborate; potassium carbonate; palladium diacetate; trimethylpyruvic acid / N,N-dimethyl acetamide / 36 h / 100 °C / Inert atmosphere
3: dihydrogen peroxide; potassium carbonate / water; dimethyl sulfoxide / 12 h / 20 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); tricyclohexylphosphine tetrafluoroborate; dihydrogen peroxide; palladium diacetate; sodium carbonate; potassium carbonate; trimethylpyruvic acid;
In
1,4-dioxane; N,N-dimethyl acetamide; water; dimethyl sulfoxide;
1: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2012.10.048