Boc-Leu-Aib-Phe-Phe-OH

Base Information

Chemical Name:Boc-Leu-Aib-Phe-Phe-OH
CAS No.:1371636-49-5
Molecular Formula:C₃₃H₄₆N₄O₇
Molecular Weight:610.751
Hs Code.:

Synonyms:Boc-Leu-Aib-Phe-Phe-OH

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Chemical Property of Boc-Leu-Aib-Phe-Phe-OH

Chemical Property:

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Technology Process of Boc-Leu-Aib-Phe-Phe-OH

There total 8 articles about Boc-Leu-Aib-Phe-Phe-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1371636-48-4
Boc-Leu-Aib-Phe-Phe-OMe

: 1371636-49-5
Boc-Leu-Aib-Phe-Phe-OH

Guidance literature:: Boc-Leu-Aib-Phe-Phe-OMe; With water; sodium hydroxide; In methanol; for 10h;

With hydrogenchloride; In water; pH=2;
DOI:10.1039/c1sm05958k

Reference yield:

: 87208-83-1
N-tert-butoxycarbonyl-L-leucyl-α-methylalanine methyl ester

: 1371636-49-5
Boc-Leu-Aib-Phe-Phe-OH

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; sodium hydroxide / methanol / 10 h

1.2: pH 2

2.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane; ethyl acetate / 20 °C / Cooling with ice

3.1: water; sodium hydroxide / methanol / 10 h

3.2: pH 2

4.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Cooling with ice

5.1: water; sodium hydroxide / methanol / 10 h

5.2: pH 2

With water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; dichloromethane; ethyl acetate;
DOI:10.1039/c1sm05958k

Reference yield:

: 72485-34-8
Boc-Leu-Aib-OH

: 1371636-49-5
Boc-Leu-Aib-Phe-Phe-OH

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane; ethyl acetate / 20 °C / Cooling with ice

2.1: water; sodium hydroxide / methanol / 10 h

2.2: pH 2

3.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Cooling with ice

4.1: water; sodium hydroxide / methanol / 10 h

4.2: pH 2

With water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; dichloromethane; ethyl acetate;
DOI:10.1039/c1sm05958k