1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Base Information

• Chemical Name: 1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside
• CAS No.: 103931-54-0
• Molecular Formula: C₆₁H₆₄O₁₁
• Molecular Weight: 973.173

Synonyms:1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Chemical Property of 1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of 1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

There total 8 articles about 1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1',2,3,3',4,4',6-hepta-O-benzyl-6'-O-tert-butyldiphenylsilyl-sucrose (136215-68-4) → 1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (103931-54-0)

Guidance literature:

With methanol; bromine; for 0.416667h; Heating;

DOI:10.1055/s-2001-15136

Reference yield: 78.0%

1,3,4-tri-O-benzyl-6-O-trityl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (103931-53-9) → 1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (103931-54-0)

Guidance literature:

With trifluoroacetic acid; In chloroform; water; for 0.333333h; Ambient temperature;

DOI:10.1016/S0008-6215(00)90395-1

Reference yield:

1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (1206803-49-7) → 1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (103931-54-0)

Guidance literature:

With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/ol902717y

upstream raw materials:

1,3,4-tri-O-benzyl-6-O-trityl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

1',2,3,3',4,4',6-hepta-O-benzyl-6'-O-tert-butyldiphenylsilyl-sucrose

benzyl bromide

benzyl chloride

Downstream raw materials:

1',2,3,3',4,4',6-hepta-O-benzyl-6'-O-methacryloyl-sucrose

1,3,4-tri-O-benzyl-7-deoxy-(β-D-altro,α-L-galacto)-hept-2-ulofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

1',2,3,3',4,4',6-hepta-O-benzyl-6'-O-(4-vinylbenzyl)sucrose

6-O-acetyl-1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

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