6H-Furo[3,4-c]pyrazol-6-one,3,3a,4,6a-tetrahydro-4-methoxy-(9CI)

Base Information

Chemical Name:6H-Furo[3,4-c]pyrazol-6-one,3,3a,4,6a-tetrahydro-4-methoxy-(9CI)
CAS No.:157904-76-2
Molecular Formula:C₆H₈N₂O₃
Molecular Weight:156.141
Hs Code.:
Mol file:157904-76-2.mol

Synonyms:6H-Furo[3,4-c]pyrazol-6-one,3,3a,4,6a-tetrahydro-4-methoxy-(9CI)

Suppliers and Price of 6H-Furo[3,4-c]pyrazol-6-one,3,3a,4,6a-tetrahydro-4-methoxy-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 6H-Furo[3,4-c]pyrazol-6-one,3,3a,4,6a-tetrahydro-4-methoxy-(9CI)

Chemical Property:

Boiling Point:305.6±42.0 °C(Predicted)
PSA：60.25000
Density:1.71±0.1 g/cm3(Predicted)
LogP:-1.16250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6H-Furo[3,4-c]pyrazol-6-one,3,3a,4,6a-tetrahydro-4-methoxy-(9CI)

There total 2 articles about 6H-Furo[3,4-c]pyrazol-6-one,3,3a,4,6a-tetrahydro-4-methoxy-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 10449-66-8
5-methoxyfuran-2(5H)-one

: 108858-40-8,108943-26-6,157904-76-2
(3aS,4R,6aR)-4-Methoxy-3,3a,4,6a-tetrahydro-furo[3,4-c]pyrazol-6-one

: 108858-40-8,108943-26-6,157904-76-2
(3aS,4S,6aR)-4-Methoxy-3,3a,4,6a-tetrahydro-furo[3,4-c]pyrazol-6-one

Guidance literature:: In diethyl ether; at -10 ℃; for 12h; Yield given. Yields of byproduct given;

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 10449-66-8
5-methoxyfuran-2(5H)-one

: 108858-40-8,108943-26-6,157904-76-2
(3aS,4R,6aR)-4-Methoxy-3,3a,4,6a-tetrahydro-furo[3,4-c]pyrazol-6-one

: 108858-40-8,108943-26-6,157904-76-2
(3aS,4S,6aR)-4-Methoxy-3,3a,4,6a-tetrahydro-furo[3,4-c]pyrazol-6-one

Guidance literature:: In diethyl ether; at -10 ℃; for 12h; Yield given. Yields of byproduct given;

Reference yield:

: 108858-40-8,108943-26-6,157904-76-2
(3aS,4R,6aR)-4-Methoxy-3,3a,4,6a-tetrahydro-furo[3,4-c]pyrazol-6-one

: 180576-33-4
4-isopropil-5-metoxi-2(5H)-furanona

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 6 h / Irradiation

2: 16 percent / ethyl acetate; diethyl ether; ethylbenzene / -10 °C

3: acetonitrile / 7 h / Irradiation

In diethyl ether; ethylbenzene; ethyl acetate; acetonitrile;