methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate

Base Information

Chemical Name:methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate
CAS No.:679789-16-3
Molecular Formula:C₁₉H₂₂N₂O₃
Molecular Weight:326.395
Hs Code.:

Synonyms:methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate

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Chemical Property of methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate

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Technology Process of methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate

There total 3 articles about methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 679789-05-0
methyl (2Z)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbut-2-enoate

: 679789-16-3
methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate

Guidance literature:: With hydrogen; platinum(IV) oxide; In tetrahydrofuran; for 48h; under 4654.33 Torr;
DOI:10.1021/ja038812t

Reference yield:

: 6485-52-5
L-phenylglycine amide

: 679789-16-3
methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / acetic acid / propan-2-ol / 18 h / 50 °C

2: 88 percent / H₂ / PtO₂ / tetrahydrofuran / 48 h / 4654.33 Torr

With hydrogen; acetic acid; platinum(IV) oxide; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1021/ja038812t

Reference yield:

: 37779-49-0
methyl 3-oxo-4-phenylbutanoate

: 679789-16-3
methyl (3R)-3-{[(1S)-2-amino-2-oxo-1-phenylethyl]amino}-4-phenylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / acetic acid / propan-2-ol / 18 h / 50 °C

2: 88 percent / H₂ / PtO₂ / tetrahydrofuran / 48 h / 4654.33 Torr

With hydrogen; acetic acid; platinum(IV) oxide; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1021/ja038812t