ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate

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Chemical Name:ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate
CAS No.:1441058-46-3
Molecular Formula:C₂₄H₂₈N₂O₆
Molecular Weight:440.496
Hs Code.:

Synonyms:ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate

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Chemical Property of ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate

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Technology Process of ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate

There total 5 articles about ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1441058-44-1
ethyl 2-amino-2-methyl-4-oxo-4-p-tolylbutanoate

: 61916-60-7
3-((4-methoxyphenyl)amino)-3-oxopropanoic acid

: 1441058-46-3
ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate

Guidance literature:: 3-((4-methoxyphenyl)amino)-3-oxopropanoic acid; With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

ethyl 2-amino-2-methyl-4-oxo-4-p-tolylbutanoate; With pyridine; In dichloromethane; at 20 ℃; for 2.5h;

Reference yield:

: 1441058-42-9
(E)-ethyl 2-methyl-4-oxo-4-p-tolylbut-2-enoate

: 1441058-46-3
ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium hydroxide / dimethyl sulfoxide / 20 °C

2.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

2.2: 2.5 h / 20 °C

With ammonium hydroxide; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1777-53-3
1-(p-tolyl)-2-(triphenylphosphoranylidene)ethanone

: 1441058-46-3
ethyl 2-(3-(4-methoxyphenylamino)-3-oxopropanamido)-2-methyl-4-oxo-4-p-tolylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0.33 h / 150 °C / Microwave irradiation

2.1: ammonium hydroxide / dimethyl sulfoxide / 20 °C

3.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

3.2: 2.5 h / 20 °C

With ammonium hydroxide; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;