1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate

Base Information

Chemical Name:1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate
CAS No.:387355-52-4
Molecular Formula:C₄H₄O₄*C₁₁H₁₈N₂O₂
Molecular Weight:326.349
Hs Code.:

Synonyms:1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate

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Chemical Property of 1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate

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Technology Process of 1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate

There total 2 articles about 1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-methyl-2-methoxy-2-(m-methoxyphenyl)-N-nitroso-ethylamine

: 387356-02-7
2-methylamino-N-nitroso-1-(m-methoxyphenyl)-1-ethanol

: 92188-48-2
1-(3-methoxyphenyl)-2-methylaminoethanol chlorhydrate

: 387355-52-4
1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate

Guidance literature:: With LiAlH₄; acetic acid; sodium nitrite; In tetrahydrofuran; methanol; water;

Reference yield:

: N-methyl-2-methoxy-2-(m-methoxyphenyl)-N-nitroso-ethylamine

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 387355-52-4
1-[2-methoxy-2-(3-methoxyphenyl)ethyl]-1-methylhydrazine hydrogen fumarate

Guidance literature:: N-methyl-2-methoxy-2-(m-methoxyphenyl)-N-nitroso-ethylamine; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; Cooling with ice;

(2E)-but-2-enedioic acid; In diethyl ether; ethanol;
DOI:10.1021/jm100337z