methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate

Base Information

Chemical Name:methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate
CAS No.:1351163-96-6
Molecular Formula:C₁₈H₁₈ClNO₄
Molecular Weight:347.798
Hs Code.:

Synonyms:methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate

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Chemical Property of methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate

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Technology Process of methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate

There total 4 articles about methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1351163-95-5
methyl (3-{[4-(acetyloxy)-2,6-dimethylbenzoyl]amino}-4-chlorophenyl)acetate

: 1351163-96-6
methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate

Guidance literature:: methyl (3-{[4-(acetyloxy)-2,6-dimethylbenzoyl]amino}-4-chlorophenyl)acetate; With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; methanol; water; ethyl acetate;
DOI:10.1016/j.bmc.2011.08.065

Reference yield:

: 1351163-93-3
4-(acetyloxy)-2,6-dimethylbenzoic acid

: 1351163-96-6
methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 1 h / 40 °C

2: pyridine / dichloromethane / 40 °C

3: potassium carbonate / tetrahydrofuran; methanol / 2 h / 20 °C

With pyridine; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.bmc.2011.08.065

Reference yield:

: 1351163-94-4
4-(chlorocarbonyl)-3,5-dimethylphenyl acetate

: 1351163-96-6
methyl {4-chloro-3-[(4-hydroxy-2,6-dimethylbenzoyl)amino]phenyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 40 °C

2: potassium carbonate / tetrahydrofuran; methanol / 2 h / 20 °C

With pyridine; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.08.065