tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate

Base Information

Chemical Name:tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate
CAS No.:1204595-13-0
Molecular Formula:C₂₃H₂₆O₅
Molecular Weight:382.456
Hs Code.:

Synonyms:tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate

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Technology Process of tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate

There total 1 articles about tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1204595-12-9
tert-butyl 2-iodo-5-(phenoxymethyl)benzoate

: 140-88-5,9003-32-1
ethyl acrylate

: 1204595-13-0
tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine; In dimethyl sulfoxide; for 5h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmc.2009.11.023

Reference yield: 100.0%

: 1204595-13-0
tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate

: 1204595-14-1
tert-butyl 2-(3-ethoxy-3-oxopropyl)-5-(phenoxymethyl)benzoate

Guidance literature:: tert-butyl 2-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-5-(phenoxymethyl)benzoate; With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In tetrahydrofuran; methanol; at 0 ℃; for 1h; Inert atmosphere;

With water; In tetrahydrofuran; methanol; acetone; Inert atmosphere;
DOI:10.1016/j.bmc.2009.11.023