N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

Base Information

Chemical Name:N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide
CAS No.:942996-48-7
Molecular Formula:C₂₆H₄₄N₄O₅
Molecular Weight:492.659
Hs Code.:

N<sub>1</sub>'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

Synonyms:N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

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Chemical Property of N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

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Technology Process of N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

There total 4 articles about N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 942996-45-4
C₃₁H₅₂N₄O₇

: 942996-48-7
N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 2h;
DOI:10.1021/jo070525a

Reference yield:

: 942996-41-0
N₃'-Boc-4,6-bis(octyloxy)benzene-1,3-dihydrazide

: 942996-48-7
N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 94.6 percent / Et₃N / CH₂Cl₂ / 5 h / 20 °C

2: 84 percent / HCl / ethyl acetate / 2 h

With hydrogenchloride; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1021/jo070525a

Reference yield:

: 267897-57-4
dimethyl 4,6-bis(octyloxy)-1,3-benzenedicarboxylate

: 942996-48-7
N₁'-acetyl-4,6-bis(octyloxy)benzene-1,3-dihydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / hydrazine monohydrate / methanol / 10 h / Heating

2: 60 percent / CH₂Cl₂ / 24 h / 20 °C

3: 94.6 percent / Et₃N / CH₂Cl₂ / 5 h / 20 °C

4: 84 percent / HCl / ethyl acetate / 2 h

With hydrogenchloride; hydrazine hydrate; triethylamine; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jo070525a