(E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate

Base Information

Chemical Name:(E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate
CAS No.:1372807-09-4
Molecular Formula:C₂₈H₃₀N₂O₅S
Molecular Weight:506.623
Hs Code.:

Synonyms:(E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate

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Technology Process of (E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate

There total 4 articles about (E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₈N₂O₆S

: 1372807-09-4
(E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 0 - 25 ℃; for 1.5h;
DOI:10.1002/anie.201107877

Reference yield:

: 1372807-08-3
(E)-N-cyanomethyl-4-methyl-N-(4-tetrahydro-2H-pyran-2-yloxybut-2-en-1-yl)benzenesulfonamide

: 1372807-09-4
(E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 - 25 °C

2: triethylamine / tetrahydrofuran / 3 h / 0 °C

3: toluene-4-sulfonic acid / methanol / 1.5 h / 0 - 25 °C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/anie.201107877

Reference yield:

: C₁₈H₂₈N₂O₄S

: 1372807-09-4
(E)-9H-fluoren-9-ylmethyl 2-(N-(4-hydroxybut-2-en-1-yl)-4-methylphenylsulfonamidoethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3 h / 0 °C

2: toluene-4-sulfonic acid / methanol / 1.5 h / 0 - 25 °C

With toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201107877