C₆H₁₀N₄O

Base Information

• Chemical Name: C₆H₁₀N₄O
• CAS No.: 1269473-08-6
• Molecular Formula: C₆H₁₀N₄O
• Molecular Weight: 154.172
• Mol file: 1269473-08-6.mol

Synonyms:C₆H₁₀N₄O

Chemical Property of C₆H₁₀N₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₁₀N₄O

There total 1 articles about C₆H₁₀N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-Pyroglutaminol (17342-08-4) → C6H10N4O (1269473-08-6)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / 0 °C

2: sodium azide / N,N-dimethyl-formamide / 80 °C

3: dichloromethane / 17 h / 23 °C / Inert atmosphere

With sodium azide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/asia.201000617

Reference yield:

C6H10N4O (1269473-08-6) → (S)-2-mesityl-5-((2-phenyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride (1269473-30-4)

Guidance literature:

Multi-step reaction with 4 steps

1: methanol / 2 h / 50 °C

2: hydrogenchloride; chlorobenzene / 1,4-dioxane / 0.83 h / 100 °C / Inert atmosphere

3: ammonium chloride; zinc / ethanol; water / 1 h / 20 °C

4: acetic acid / methanol / 50 °C / Inert atmosphere

With hydrogenchloride; ammonium chloride; acetic acid; chlorobenzene; zinc; In 1,4-dioxane; methanol; ethanol; water; 4: Paal-Knorr pyrrole synthesis;

DOI:10.1002/asia.201000617

Reference yield:

C6H10N4O (1269473-08-6) → (S)-5-(azidomethyl)-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride (1269473-11-1)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 2 h / 50 °C

2: hydrogenchloride; chlorobenzene / 1,4-dioxane / 0.83 h / 100 °C / Inert atmosphere

With hydrogenchloride; chlorobenzene; In 1,4-dioxane; methanol;

DOI:10.1002/asia.201000617

upstream raw materials:

(S)-Pyroglutaminol

Downstream raw materials:

(S)-5-(azidomethyl)-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

(S)-5-(aminomethyl)-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

C₁₅H₂₀N₃O⁽¹⁺⁾*Cl^(1-)

(S)-2-mesityl-5-((2-methyl-5-phenyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride