tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate

Base Information

Chemical Name:tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate
CAS No.:1237515-91-1
Molecular Formula:C₃₃H₃₂BrNO₅
Molecular Weight:602.525
Hs Code.:

Synonyms:tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate

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Chemical Property of tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate

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Technology Process of tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate

There total 4 articles about tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237517-63-3
4-acetoxy-2-(benzyloxy)benzoic acid

: 1237515-91-1
tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C / Cooling with ice

2.1: pyridine / dichloromethane / 3.33 h / 20 °C / Cooling with ice

3.1: water; sodium hydroxide / 1,4-dioxane / 2 h / 50 - 55 °C

3.2: 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 1.75 h / 120 °C

With pyridine; oxalyl dichloride; water; potassium carbonate; sodium hydroxide; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 890316-40-2
tert-butyl 2-amino-4-phenylbenzoate

: 1237515-91-1
tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 3.33 h / 20 °C / Cooling with ice

2.1: water; sodium hydroxide / 1,4-dioxane / 2 h / 50 - 55 °C

2.2: 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 1.75 h / 120 °C

With pyridine; water; potassium carbonate; sodium hydroxide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1237520-20-5
tert-butyl 2-(4-acetoxy-2-(benzyloxy)benzamido)-4-phenylbenzoate

: 1237515-91-1
tert-butyl 2-(2-(benzyloxy)-4-(2-bromoethoxy)benzamido)-4-phenylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / 1,4-dioxane / 2 h / 50 - 55 °C

1.2: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 1.75 h / 120 °C

With water; potassium carbonate; sodium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;