(E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol

Base Information

Chemical Name:(E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol
CAS No.:1612146-72-1
Molecular Formula:C₂₀H₂₇N₃O₂S
Molecular Weight:373.519
Hs Code.:

Synonyms:(E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol

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Chemical Property of (E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol

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Technology Process of (E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol

There total 6 articles about (E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 458-36-6
trans-coniferyl aldehyde

: 104617-86-9
2-amino-4,5,6,7-tetrahydro-6-propylaminobenzothiazole

: 1612146-72-1
(E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol

Guidance literature:: trans-coniferyl aldehyde; 2-amino-4,5,6,7-tetrahydro-6-propylaminobenzothiazole; In dichloromethane; for 1h;

With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 48h;

Reference yield:

: 4046-02-0
ethyl 4-hydroxy-3-methoxycinnamate

: 1612146-72-1
(E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran / 6 h / -10 - 20 °C

3.1: manganese(IV) oxide / dichloromethane / 24 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

5.1: dichloromethane / 1 h

5.2: 48 h / 20 °C

With 1H-imidazole; manganese(IV) oxide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1485529-16-5
(E)-ethyl 3-(4-((tert-butyldimethylsilyl)oxy)-3-methoxyphenyl)acrylate

: 1612146-72-1
(E)-4-(3-((2-amino-4,5,6,7-tetrahydrobenzo[d] thiazol-6-yl)(propyl)amino)prop-1-en-1-yl)-2-methoxyphenol

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran / 6 h / -10 - 20 °C

2.1: manganese(IV) oxide / dichloromethane / 24 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

4.1: dichloromethane / 1 h

4.2: 48 h / 20 °C

With manganese(IV) oxide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane;