27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁹⁾,11,13,15⁽³⁰⁾,25,27-hexaen-29-ol

Base Information

• Chemical Name: 27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁹⁾,11,13,15⁽³⁰⁾,25,27-hexaen-29-ol
• CAS No.: 113858-78-9
• Molecular Formula: C₃₂H₃₈N₄O₁₃
• Molecular Weight: 686.673

Synonyms:27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁹⁾,11,13,15⁽³⁰⁾,25,27-hexaen-29-ol

Chemical Property of 27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁹⁾,11,13,15⁽³⁰⁾,25,27-hexaen-29-ol

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Technology Process of 27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁹⁾,11,13,15⁽³⁰⁾,25,27-hexaen-29-ol

There total 5 articles about 27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁹⁾,11,13,15⁽³⁰⁾,25,27-hexaen-29-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-bis-bromomethyl-2,5-dimethoxy-benzene (72652-35-8) → 27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.111,15]triaconta-1(29),11,13,15(30),25,27-hexaen-29-ol (113858-78-9)

Guidance literature:

Multi-step reaction with 4 steps

1: NaH / tetrahydrofuran

2: Ce(NH₄)2(NO₃)6 / acetonitrile; H₂O

3: H₂SO₄ / ethanol; CH₂Cl₂

With ammonium cerium(IV) nitrate; sulfuric acid; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;

DOI:10.1021/ja00217a047

Reference yield:

2,6-bis-(7-hydroxy-2,5-dioxaheptyl)-1,4-dimethoxybenzene (113858-79-0) → 27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.111,15]triaconta-1(29),11,13,15(30),25,27-hexaen-29-ol (113858-78-9)

Guidance literature:

Multi-step reaction with 4 steps

1: NaH / tetrahydrofuran

2: Ce(NH₄)2(NO₃)6 / acetonitrile; H₂O

3: H₂SO₄ / ethanol; CH₂Cl₂

With ammonium cerium(IV) nitrate; sulfuric acid; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;

DOI:10.1021/ja00217a047

Reference yield:

27,29-Dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.111,15]triaconta-1(28),11,14,25(29),26-pentaene-13,30-dione (113858-85-8) → 27-(2,4-Dinitro-phenylazo)-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.111,15]triaconta-1(29),11,13,15(30),25,27-hexaen-29-ol (113858-78-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄ / ethanol; CH₂Cl₂

With sulfuric acid; In ethanol; dichloromethane;

DOI:10.1021/ja00217a047

upstream raw materials:

27-[(2,4-Dinitro-phenyl)-hydrazono]-13,30-dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁸⁾,11,13,15⁽³⁰⁾,25-pentaen-29-one

1,3-bis-bromomethyl-2,5-dimethoxy-benzene

2,6-bis-(7-hydroxy-2,5-dioxaheptyl)-1,4-dimethoxybenzene

27,29-Dimethoxy-3,6,9,17,20,23-hexaoxa-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁸⁾,11,14,25⁽²⁹⁾,26-pentaene-13,30-dione

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