2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride

Base Information

Chemical Name:2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride
CAS No.:1400562-67-5
Molecular Formula:C₂₂H₂₃ClFN₃O₅
Molecular Weight:463.893
Hs Code.:

Synonyms:2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride

Suppliers and Price of 2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride

There total 2 articles about 2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1400562-27-7
phenyl 2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-1-thio-β-D-glucopyranoside

: 1400562-67-5
2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride

: 1400562-68-6
2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-β-D-galactopyranosyl fluoride

Guidance literature:: With N-ethyl-N-(trifluoromethylsulfanyl)ethanamine; In 1,2-dichloro-ethane; at 0 - 60 ℃; for 39h; Overall yield = 94 %; Inert atmosphere;
DOI:10.1016/j.carres.2012.07.003

Reference yield:

: 277756-87-3
phenyl 2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

: 1400562-67-5
2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl fluoride

: 1400562-68-6
2-azido-3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-β-D-galactopyranosyl fluoride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1,2-dichloro-ethane / 2 h / 0 - 20 °C

2: N-ethyl-N-(trifluoromethylsulfanyl)ethanamine / 1,2-dichloro-ethane / 39 h / 0 - 60 °C / Inert atmosphere

With pyridine; N-ethyl-N-(trifluoromethylsulfanyl)ethanamine; In 1,2-dichloro-ethane;
DOI:10.1016/j.carres.2012.07.003