2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose
CAS No.:831209-71-3
Molecular Formula:C₅₃H₄₄O₁₆
Molecular Weight:936.923
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose

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Chemical Property of 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose

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Technology Process of 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose

There total 4 articles about 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 831209-68-8
allyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3-O-benzoyl-α-D-mannopyranoside

: 831209-71-3
2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 20 °C

2: 85 percent / PdCl₂ / methanol / 2 h / 20 °C

With pyridine; palladium dichloride; In methanol;
DOI:10.1016/j.bmc.2004.09.049

Reference yield:

: 831209-66-6
allyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3-O-benzoyl-4,6-O-benzylidene-α-D-mannopyranoside

: 831209-71-3
2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / CH₃COOH / H₂O / 2 h / 70 °C

2: 80 percent / pyridine / 20 °C

3: 85 percent / PdCl₂ / methanol / 2 h / 20 °C

With pyridine; acetic acid; palladium dichloride; In methanol; water;
DOI:10.1016/j.bmc.2004.09.049

Reference yield:

: 502765-04-0
2,3,4-tri-O-benzoyl-α,β-D-xylopyranosyl trichloroacetimidate

: 831209-71-3
2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzoyl-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / -20 - 0 °C

2: 90 percent / CH₃COOH / H₂O / 2 h / 70 °C

3: 80 percent / pyridine / 20 °C

4: 85 percent / PdCl₂ / methanol / 2 h / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; acetic acid; palladium dichloride; In methanol; dichloromethane; water;
DOI:10.1016/j.bmc.2004.09.049