OsH(CO)2(P(C₆H₅)3)3⁽¹⁺⁾*BF₄^(1-)=[OsH(CO)2(P(C₆H₅)3)3]BF₄

Base Information

• Chemical Name: OsH(CO)2(P(C₆H₅)3)3⁽¹⁺⁾*BF₄^(1-)=[OsH(CO)2(P(C₆H₅)3)3]BF₄
• CAS No.: 82433-97-4
• Molecular Formula: BF₄*C₅₆H₄₆O₂OsP₃
• Molecular Weight: 1120.91

Synonyms:OsH(CO)2(P(C₆H₅)3)3⁽¹⁺⁾*BF₄^(1-)=[OsH(CO)2(P(C₆H₅)3)3]BF₄

Chemical Property of OsH(CO)2(P(C₆H₅)3)3⁽¹⁺⁾*BF₄^(1-)=[OsH(CO)2(P(C₆H₅)3)3]BF₄

Chemical Property:

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Technology Process of OsH(CO)2(P(C₆H₅)3)3⁽¹⁺⁾*BF₄^(1-)=[OsH(CO)2(P(C₆H₅)3)3]BF₄

There total 1 articles about OsH(CO)2(P(C₆H₅)3)3⁽¹⁺⁾*BF₄^(1-)=[OsH(CO)2(P(C₆H₅)3)3]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.6%

tetrafluoroboric acid + carbonyldihydridotris(triphenylphosphine)osmium (36179-61-0,12104-84-6) → OsH(CO)2(P(C6H5)3)3(1+)*BF4(1-)=[OsH(CO)2(P(C6H5)3)3]BF4 (82433-97-4)

Guidance literature:

With carbon monoxide; water; In methanol; dichloromethane; byproducts: H2; Os-complex was heated in a soln. comprised of CH2Cl2, MeOH and aq. HBF4, heated under CO to 80°C for 1.5 h; H2O was added, recrystd. from EtOH; elem. anal.;

DOI:10.1016/S0022-328X(00)81955-5

Reference yield: 94.8%

OsH(CO)2(P(C6H5)3)3(1+)*BF4(1-)=[OsH(CO)2(P(C6H5)3)3]BF4 (82433-97-4) → Os(CO)2(PPh3)3 (35880-55-8,64479-09-0)

Guidance literature:

With sodium hydroxide; triphenylphosphine; In methanol; byproducts: HClO4; a soln. of Os-complex in MeOH was heated to boiling under N2, NaOH and PPh3 were added, heated under reflux for 1 h; filtered, washed with EtOH and hexane, recrystd. from C6H6-petroleum spirit; elem. anal.;

DOI:10.1016/S0022-328X(00)81955-5

upstream raw materials:

carbonyldihydridotris(triphenylphosphine)osmium

Downstream raw materials:

Os(CO)2(PPh₃)3

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