N,N'-dinitroso-1,4-phenylenedihydroxylamine

Base Information

• Chemical Name: N,N'-dinitroso-1,4-phenylenedihydroxylamine
• CAS No.: 24924-26-3
• Molecular Formula: C₆H₆N₄O₄
• Molecular Weight: 198.138
• Mol file: 24924-26-3.mol

Synonyms:N,N'-dinitroso-1,4-phenylenedihydroxylamine

Chemical Property of N,N'-dinitroso-1,4-phenylenedihydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-dinitroso-1,4-phenylenedihydroxylamine

There total 1 articles about N,N'-dinitroso-1,4-phenylenedihydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-Benzochinondioxim (105-11-3,6133-83-1,6421-98-3) → N,N'-dinitroso-1,4-phenylenedihydroxylamine (24924-26-3)

Guidance literature:

Multistep reaction; (i) NO, NaOMe, MeOH, (ii) HCl;

DOI:10.1021/jo01067a072

Reference yield: 94.0%

manganese(II) sulfate + N,N'-dinitroso-1,4-phenylenedihydroxylamine (24924-26-3) → Mn(2+)*C6H4N4O4(2-)*H2O=Mn(C6H4N4O4)*H2O

Guidance literature:

In water; drying in air at 110°C;

DOI:10.1016/0022-1902(70)80641-8

Reference yield:

N,N'-dinitroso-1,4-phenylenedihydroxylamine (24924-26-3) → p-dinitrosobenzene (105-12-4,9003-34-3)

Guidance literature:

(heating);

DOI:10.1021/jo01067a072

upstream raw materials:

1,4-Benzochinondioxim

Downstream raw materials:

p-dinitrosobenzene