(1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

Base Information

Chemical Name:(1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime
CAS No.:136838-55-6
Molecular Formula:C₁₆H₁₉NO₃
Molecular Weight:273.332
Hs Code.:

Synonyms:(1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

Suppliers and Price of (1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

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Technology Process of (1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

There total 1 articles about (1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136838-50-1
(1R,2S,4S,7R)-7-Benzyloxymethyl-2-bromo-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde

: 136838-55-6
(1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

Guidance literature:: With hydroxylamine; at 23 ℃; for 8h;
DOI:10.1021/ja00023a066

Reference yield:

: 136838-55-6
(1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

: (1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbonitrile

Guidance literature:: With pyridine; p-toluenesulfonyl chloride; at 23 ℃; for 2h;
DOI:10.1021/ja00023a066

Reference yield:

: 136838-55-6
(1R,2S,4S,7R)-7-Benzyloxymethyl-2-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde oxime

: 53153-20-1
(1R,4S,7R)-(-)-bicyclo <2.2.1> hept-7-benzyloxymethyl-5-ene-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: TsCl, pyridine / 2 h / 23 °C

2: 1 M aq. NaOH / 1 h / 23 °C

With pyridine; sodium hydroxide; p-toluenesulfonyl chloride;
DOI:10.1021/ja00023a066