2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile

Base Information

• Chemical Name: 2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile
• CAS No.: 1026787-40-5
• Molecular Formula: C₁₆H₂₁N₃Si₂
• Molecular Weight: 311.534

Synonyms:2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile

Chemical Property of 2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile

Chemical Property:

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Technology Process of 2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile

There total 2 articles about 2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

bis(trimethylsilylethynyl)ketone (60836-10-4) + malononitrile (109-77-3) → 2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile (1026787-40-5)

Guidance literature:

With triethylamine; In toluene; at 120 ℃; for 2h;

DOI:10.1021/jo800260b

Reference yield: 70.0%

bis(trimethylsilylethynyl)ketone (60836-10-4) + malononitrile (109-77-3) → 2-amino-4-(trimethylsilylethynyl)-6-(trimethylsilyl)benzene-1,3-dicarbonitrile (1026787-40-5) + 2,5-diamino-7-(trimethylsilyl)naphthalene-1,3,6-tricarbonitrile (1071082-30-8) + 2,9-diamino-5,7-bis(trimethylsilyl)benzo[a]pyrimido[2,1,6-cd]-pyrrolizine-3,4,8-tricarbonitrile (1071082-28-4)

Guidance literature:

With triethylamine; In toluene; at 120 ℃; for 2h;

DOI:10.1016/j.tet.2008.07.084

upstream raw materials:

bis(trimethylsilylethynyl)ketone

malononitrile

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