C₄₁H₅₆O₄

Base Information

• Chemical Name: C₄₁H₅₆O₄
• CAS No.: 1426539-27-6
• Molecular Formula: C₄₁H₅₆O₄
• Molecular Weight: 612.893
• Mol file: 1426539-27-6.mol

Synonyms:C₄₁H₅₆O₄

Chemical Property of C₄₁H₅₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₄₁H₅₆O₄

There total 1 articles about C₄₁H₅₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

cis-Octadecenoic acid (112-80-1,2027-47-6) + 1-methoxy-3-(trityloxy)propan-2-ol (106972-46-7) → C41H56O4 (1426539-27-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1016/j.bmcl.2013.01.002

Reference yield:

C41H56O4 (1426539-27-6) → sodium?O-3-methoxy-2-((Z)-oleoyloxy)propyl?O-hydrogen phosphorothioate (1426539-21-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2.1: 1H-tetrazole / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: sulfur; carbon disulfide; pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: tert-butylamine; N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / Inert atmosphere

4.2: Dowex 50WX₈-200 resin neutral Na⁺ form

With pyridine; 1H-tetrazole; carbon disulfide; N,O-bis-(trimethylsilyl)-acetamide; sulfur; tert-butylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;

DOI:10.1016/j.bmcl.2013.01.002

upstream raw materials:

cis-Octadecenoic acid

1-methoxy-3-(trityloxy)propan-2-ol

Downstream raw materials:

sodium?O-3-methoxy-2-((Z)-oleoyloxy)propyl?O-hydrogen phosphorothioate