Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid

Base Information

Chemical Name:Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid
CAS No.:139493-97-3
Molecular Formula:C₃₈H₅₄O₆Si
Molecular Weight:634.929
Hs Code.:

Synonyms:Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid

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Technology Process of Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid

There total 4 articles about Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 139493-96-2
Octyl-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

: 58479-61-1
tert-butylchlorodiphenylsilane

: 139493-97-3
Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

Reference yield:

: 139493-94-0
Octyl-3,6-di-O-allyl-2-O-benzyl-β-D-mannopyranosid

: 139493-97-3
Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH / 1) DMF, 15 min, 2) 2.5 h

2: 2) HgCl₂, HgO / 1) 2)2>PF₆, H₂ / 1) THF, 10 min, r.t., 2) acetone, water, 30 min

3: 92 percent / imidazole / dimethylformamide / 1 h / 0 °C

With 1H-imidazole; sodium hydride; mercury dichloride; mercury(II) oxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; hydrogen; In N,N-dimethyl-formamide;

Reference yield:

: 139493-95-1
Octyl-3,6-di-O-allyl-2-O-benzyl-4-O-methyl-β-D-mannopyranosid

: 139493-97-3
Octyl-2-O-benzyl-6-O-tert-butyldiphenylsilyl-4-O-methyl-β-D-mannopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 2) HgCl₂, HgO / 1) 2)2>PF₆, H₂ / 1) THF, 10 min, r.t., 2) acetone, water, 30 min

2: 92 percent / imidazole / dimethylformamide / 1 h / 0 °C

With 1H-imidazole; mercury dichloride; mercury(II) oxide; (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; hydrogen; In N,N-dimethyl-formamide;