methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate

Base Information

• Chemical Name: methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate
• CAS No.: 1220117-38-3
• Molecular Formula: C₂₃H₃₄O₆
• Molecular Weight: 406.519

Synonyms:methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate

Chemical Property of methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate

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Technology Process of methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate

There total 1 articles about methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

methyl (1R,2R,4S)-2-[(E)-2-iodoethenyl]-4-(methoxymethoxy)cyclopentanecarboxylate (1020414-84-9) + C20H31BO2 → methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate (1220117-38-3)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 35 ℃;

DOI:10.1002/ejoc.200901233

Reference yield: 89.0%

methyl (1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentanecarboxylate (1220117-38-3) → {(1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentyl}methanol (1220117-26-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 - 25 ℃;

DOI:10.1002/ejoc.200901233

upstream raw materials:

methyl (1R,2R,4S)-2-[(E)-2-iodoethenyl]-4-(methoxymethoxy)cyclopentanecarboxylate

Downstream raw materials:

{(1R,2S,4S)-2-{(E)-6-[(4-methoxybenzyl)oxy]hex-1-enyl}-4-(methoxymethoxy)cyclopentyl}methanol

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