6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside)

Base Information

• Chemical Name: 6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside)
• CAS No.: 1383476-50-3
• Molecular Formula: C₅₄H₆₆O₁₂
• Molecular Weight: 907.111
• Mol file: 1383476-50-3.mol

Synonyms:6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside)

Chemical Property of 6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside)

There total 1 articles about 6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6α-O-benzoyl chlorogenin (1173241-36-5) + 3,6-di-O-benzoyl-2,4-di-O-levulinoyl-D-glucopyranosyl trichloroacetimidate (1383476-27-4) → 6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside) (1383476-50-3)

Guidance literature:

Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 20 °C / Inert atmosphere

2: hydrazinium monoacetate / 20 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; hydrazinium monoacetate; In dichloromethane;

DOI:10.1016/j.ejmech.2012.04.022

Reference yield:

2,3,4-tri-O-benzoyl-α,β-L-arabinopyranosyl trichloroacetimidate + 6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside) (1383476-50-3) → C106H106O26 (1383476-30-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; for 8.33333h; Inert atmosphere; Molecular sieve;

DOI:10.1016/j.ejmech.2012.04.022

Reference yield:

C13H18Cl3NO7 (1105054-79-2) + 6-O-benzoylchlorogenin 3-O-(3,6-di-O-benzoyl-β-D-glucopyranoside) (1383476-50-3) → C76H98O24 (1383476-32-1)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; for 8.33333h; Inert atmosphere; Molecular sieve;

DOI:10.1016/j.ejmech.2012.04.022

upstream raw materials:

6α-O-benzoyl chlorogenin

3,6-di-O-benzoyl-2,4-di-O-levulinoyl-D-glucopyranosyl trichloroacetimidate

Downstream raw materials:

C₁₀₆H₁₀₆O₂₆

C₇₆H₉₈O₂₄