C₁₅H₁₅N₃OS

Base Information

Chemical Name:C₁₅H₁₅N₃OS
CAS No.:1420626-70-5
Molecular Formula:C₁₅H₁₅N₃OS
Molecular Weight:285.37
Hs Code.:

C<sub>15</sub>H<sub>15</sub>N<sub>3</sub>OS

Synonyms:C₁₅H₁₅N₃OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₅N₃OS

Chemical Property:

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Technology Process of C₁₅H₁₅N₃OS

There total 13 articles about C₁₅H₁₅N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1420830-32-5
C₁₅H₁₃N₅OS

: 1420626-70-5
C₁₅H₁₅N₃OS

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 1h;

Reference yield:

: 1420830-25-6
C₁₃H₁₂N₂OS

: 1420626-70-5
C₁₅H₁₅N₃OS

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C

1.2: 2 h

2.1: osmium(VIII) oxide / water; 1,4-dioxane / 0.5 h / 20 °C

2.2: 3 h / 20 °C

3.1: caesium carbonate / ethyl acetate; ethanol / 2 h / 50 °C

4.1: methanol; sodium tetrahydroborate / 16 h / 20 °C

5.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 1 h / 20 °C

6.1: tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere

7.1: triphenylphosphine / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

7.2: 2.33 h / 0 - 20 °C

8.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 20 °C

With methanol; sodium tetrahydroborate; osmium(VIII) oxide; tetrapropylammonium perruthennate; palladium 10% on activated carbon; hydrogen; sodium hydride; caesium carbonate; 4-methylmorpholine N-oxide; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1420830-24-5
C₁₁H₉IN₂OS

: 1420626-70-5
C₁₅H₁₅N₃OS

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 90 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C

2.2: 2 h

3.1: osmium(VIII) oxide / water; 1,4-dioxane / 0.5 h / 20 °C

3.2: 3 h / 20 °C

4.1: caesium carbonate / ethyl acetate; ethanol / 2 h / 50 °C

5.1: methanol; sodium tetrahydroborate / 16 h / 20 °C

6.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 1 h / 20 °C

7.1: tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere

8.1: triphenylphosphine / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

8.2: 2.33 h / 0 - 20 °C

9.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 20 °C

With methanol; sodium tetrahydroborate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrapropylammonium perruthennate; palladium 10% on activated carbon; hydrogen; sodium hydride; caesium carbonate; 4-methylmorpholine N-oxide; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;