N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

Base Information

Chemical Name:N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane
CAS No.:75956-67-1
Molecular Formula:C₄₂H₄₂N₄O₂₀
Molecular Weight:922.81
Hs Code.:

Synonyms:N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

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Chemical Property of N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

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Technology Process of N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

There total 4 articles about N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 75956-65-9
N,N',N'',N'''-tetrakis<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10,14-tetraazatetradecane

: 75956-67-1
N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

Guidance literature:: With boron tribromide; In tetrachloromethane; dichloromethane; Ambient temperature;
DOI:10.1021/jm00134a015

Reference yield:

: 71-44-3
Spermine

: 75956-67-1
N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / tetrahydrofuran / Ambient temperature

2: 67 percent / BBr₃ / CCl₄; CH₂Cl₂ / Ambient temperature

With boron tribromide; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1021/jm00134a015

Reference yield:

: 75956-64-8
2,3-Dimethoxy-4-(methoxycarbonyl)benzoylchlorid

: 75956-67-1
N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / tetrahydrofuran / Ambient temperature

2: 67 percent / BBr₃ / CCl₄; CH₂Cl₂ / Ambient temperature

With boron tribromide; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1021/jm00134a015