dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate

Base Information

Chemical Name:dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate
CAS No.:1251849-41-8
Molecular Formula:C₃₃H₂₆O₄
Molecular Weight:486.567
Hs Code.:

Synonyms:dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate

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Chemical Property of dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate

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Technology Process of dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate

There total 2 articles about dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 64985-86-0
1-naphthoic anhydride

: 2,2-bis-(3-phenyl-prop-2-ynyl)-malonic acid dimethyl ester

: 1251849-41-8
dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate

Guidance literature:: With tris(acetonitrile)pentamethylcyclopentadienylrhodium(III) hexafluoroantimonate; copper diacetate; In N,N-dimethyl-formamide; at 140 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201500252

Reference yield: 38.0%

: 81-84-5
1,8-Naphthalic anhydride

: 2,2-bis-(3-phenyl-prop-2-ynyl)-malonic acid dimethyl ester

: 1251849-41-8
dimethyl 7,11-diphenyl-8H-cyclopenta[b]phenanthrene-9,9(10H)-dicarboxylate

Guidance literature:: With tris(acetonitrile)pentamethylcyclopentadienylrhodium(III) hexafluoroantimonate; copper diacetate; In N,N-dimethyl-formamide; at 140 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201500252