N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide

Base Information

Chemical Name:N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide
CAS No.:1075241-57-4
Molecular Formula:C₂₀H₂₅ClN₂O₂S
Molecular Weight:392.95
Hs Code.:

Synonyms:N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide

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Chemical Property of N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide

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Technology Process of N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide

There total 4 articles about N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₂₁N

: 926252-23-5
5-chloro-2-methoxybenzoyl isothiocyanate

: 1075241-57-4
N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide

Guidance literature:: C₁₁H₂₁N; 5-chloro-2-methoxybenzoyl isothiocyanate; In tetrahydrofuran; dichloromethane; for 1h;

With pyridine; iodine; In tetrahydrofuran; methanol; dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 3438-16-2
5-chloro-2-methoxybenzoic acid

: 1075241-57-4
N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / toluene / 20 °C / Heating / reflux

2.1: tetrahydrofuran; acetone / 2 h / 20 °C

3.1: tetrahydrofuran / 1 h

3.2: 1 h / 20 °C

With thionyl chloride; In tetrahydrofuran; acetone; toluene;

Reference yield:

: 40571-47-9
1-methylcyclobutan-1-amine

: 66-25-1
hexanal

: 1075241-57-4
N-[(5Z)-4-butyl-2-(1-methylcyclobutyl)-isothiazol-5(2H)-ylidene]-5-chloro-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium sulfate / dichloromethane / 1 h

2.1: tetrahydrofuran / 1 h

2.2: 1 h / 20 °C

With magnesium sulfate; In tetrahydrofuran; dichloromethane;