cyanoacetate de p-methoxybenzyle

Base Information

• Chemical Name: cyanoacetate de p-methoxybenzyle
• CAS No.: 115823-81-9
• Molecular Formula: C₁₁H₁₁NO₃
• Molecular Weight: 205.213
• Mol file: 115823-81-9.mol

Synonyms:cyanoacetate de p-methoxybenzyle

Chemical Property of cyanoacetate de p-methoxybenzyle

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyanoacetate de p-methoxybenzyle

There total 2 articles about cyanoacetate de p-methoxybenzyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

→ cyanoacetate de p-methoxybenzyle (115823-81-9)

Guidance literature:

With N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 2h;

With triethylamine; In dichloromethane; at 0 ℃;

Reference yield: 50.0%

(4-methoxyphenyl)methyl 2-isocyanoacetate → p-methoxybenzyl acetate (104-21-2) + cyanoacetate de p-methoxybenzyle (115823-81-9)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; at -78 ℃;

DOI:10.1039/a700570i

Reference yield:

(2E,4E)-5-(4-(dimethylamino)-2,6-dimethoxyphenyl)penta-2,4-dienal + cyanoacetate de p-methoxybenzyle (115823-81-9) → C26H28N2O5

Guidance literature:

With piperidine; In tetrahydrofuran; at 50 ℃;

DOI:10.1021/acschemneuro.6b00174

Downstream raw materials:

cyano-2 methyl propanoate de p-methoxybenzyle