N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline

Base Information

• Chemical Name: N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline
• CAS No.: 1227053-92-0
• Molecular Formula: C₁₆H₂₅N
• Molecular Weight: 231.381
• Mol file: 1227053-92-0.mol

Synonyms:N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline

Chemical Property of N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline

There total 1 articles about N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

para-bromotoluene (106-38-7) + 2,2-dimethyl-6-heptenyl-1-amine (138286-03-0) → N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline (1227053-92-0)

Guidance literature:

With palladium diacetate; johnphos; sodium t-butanolate; In toluene; at 80 ℃; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1002/adsc.201500287

Reference yield:

N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline (1227053-92-0) → C16H25N (1227053-94-2) + C16H25N (1227053-95-3)

Guidance literature:

With bis(indenyl)dimethyl-titanium; In toluene; at 105 ℃; for 72h; Inert atmosphere;

DOI:10.1002/anie.200906557

Reference yield:

N-(2,2-dimethyl-6-hepten-1-yl)-4-methylaniline (1227053-92-0) → C16H25N + C16H25N

Guidance literature:

With [([(2-MeAP)2Ti(NMe₂)2])2Ti(NMe₂)2]; In hexane; at 140 ℃; for 96h; Overall yield = 15 %; Overall yield = 70 mg; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1002/adsc.201500287

upstream raw materials:

para-bromotoluene

2,2-dimethyl-6-heptenyl-1-amine

Downstream raw materials:

C₁₆H₂₅N

C₁₆H₂₅N