[5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II)

Base Information

• Chemical Name: [5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II)
• CAS No.: 223903-71-7
• Molecular Formula: C₆₈H₇₅IN₄Zn
• Molecular Weight: 1140.66

Synonyms:[5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II)

Chemical Property of [5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II)

Chemical Property:

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Technology Process of [5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II)

There total 2 articles about [5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

zinc(II) acetate dihydrate (5970-45-6) + 5,10,15-Tris(3,5-di-tert-butylphenyl)-20-(4-iodophenyk)porphyrin → [5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II) (223903-71-7)

Guidance literature:

In methanol; chloroform; at 20 ℃; for 18h; Darkness;

DOI:10.1002/anie.201903654

Reference yield:

5-(4'-iodophenyl)-10,15,20-tris(3'',5''-di-tert-butylphenyl)porphyrin → [5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II) (223903-71-7)

Guidance literature:

With zinc(II) acetate dihydrate; In methanol; dichloromethane; for 1h; Reflux;

DOI:10.1002/ejoc.200900149

Reference yield: 87.0%

1-ethynyl-5-triethylsilylethynylanthracene (778649-19-7) + [5-(4-iodophenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphinato]zinc(II) (223903-71-7) → [Zn(C20N4H8)(C6H3(C(CH3)3)2)3(C6H4)CC(C14H8)CCH] (781673-39-0)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; methanol; THF:MeOH=50:50; at room temp. for 6 h;

DOI:10.1039/b406680d

upstream raw materials:

zinc(II) acetate dihydrate

Downstream raw materials:

(((C₄H₉)2C₆H₃)3C₂₀H₈N₄(C₆H₄)ZnC₂)2C₁₄H₈

[Zn(C₂₀N₄H₈)(C₆H₃(C(CH₃)3)2)3(C₆H₄)CC(C₁₄H₈)CCH]

C₁₃₅H₁₅₈N₄O₅Zn

[C₁₀H₆(C₆H₄(ZnC₂₀H₈N₄(C₆H₃(C(CH₃)3)2)3))2]

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