(1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate

Base Information

Chemical Name:(1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate
CAS No.:1009036-50-3
Molecular Formula:C₃₆H₆₀O₆Si
Molecular Weight:616.954
Hs Code.:

(1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate

Synonyms:(1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate

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Chemical Property of (1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate

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Technology Process of (1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate

There total 1 articles about (1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1009036-59-2
C₃₆H₆₂O₆Si

: 1009036-50-3
(1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jo702384d

Reference yield: 88.0%

: 1009036-50-3
(1R,2R)-1-ethyl-2-methyl-but-3-enyl (2R,3S,4R,5S,6S,8R)-3-(tert-butyldimethylsilanyloxy)-5-(4-methoxybenzyloxy)-2,4,6,8-tetramethyl-9-oxoundec-10-enoate

: 1009036-51-4
(E)-(3R,4S,5R,6S,7S,9R,13R,14R)-4-(tert-butyldimethylsilanyloxy)-14-ethyl-6-(4-methoxybenzyloxy)-3,5,7,9,13-pentamethyloxacyclotetradec-11-ene-2,10-dione

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/jo702384d