Technology Process of 11b-phenyl-1,2,3,5,6,11b-hexahydro<1>benzothieno<3,2-g>indolizine
There total 4 articles about 11b-phenyl-1,2,3,5,6,11b-hexahydro<1>benzothieno<3,2-g>indolizine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 8h;
Heating;
DOI:10.1071/CH9850765
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 89 percent / CH2Cl2 / 7 h / 0 - 5 °C
2: 82 percent / 85percent orthophosphoric acid / 1 h / 95 - 105 °C
3: 89 percent / lithium tetrahydroaluminate / tetrahydrofuran / 8 h / Heating
With
lithium aluminium tetrahydride; phosphoric acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1071/CH9850765
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 89 percent / CH2Cl2 / 7 h / 0 - 5 °C
2: 82 percent / 85percent orthophosphoric acid / 1 h / 95 - 105 °C
3: 89 percent / lithium tetrahydroaluminate / tetrahydrofuran / 8 h / Heating
With
lithium aluminium tetrahydride; phosphoric acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1071/CH9850765
