(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

Base Information

Chemical Name:(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester
CAS No.:113068-90-9
Molecular Formula:C₄₂H₅₃NO₇SSi₂
Molecular Weight:772.122
Hs Code.:

(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

Synonyms:(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

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Chemical Property of (5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

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Technology Process of (5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

There total 1 articles about (5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 113068-93-2
4-(tert-Butyl-diphenyl-silanyloxymethyl)-benzoic acid

: 88585-78-8
<4S,5R,6S(R)>-3-(hydroxymethyl)-6-<1-<(tert-butyldimethylsilyl)oxy>ethyl>-7-oxo-4-thia-1-azabicyclo<3.2.0>hept-2-enecarboxylic acid 2-allyl ester

: 113068-90-9
(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

Guidance literature:

Reference yield: 90.0%

: 113068-90-9
(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

: 113068-91-0
(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-(4-hydroxymethyl-benzoyloxymethyl)-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; for 1h;

Reference yield:

: 113068-90-9
(5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-benzoyloxymethyl]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

: 113030-48-1
C₂₂H₂₀N₂O₆S

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / -50 °C

2: Bu₄NF*3H₂O, HOAc / tetrahydrofuran

3: acetic acid, Pd(PPh₃)4, PPh₃ / CH₂Cl₂ / 0.25 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane;