trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester

Base Information

• Chemical Name: trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester
• CAS No.: 220910-81-6
• Molecular Formula: C₁₆H₁₄ClF₃N₂O₄S
• Molecular Weight: 422.812

Synonyms:trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester

Chemical Property of trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester

Chemical Property:

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Technology Process of trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester

There total 3 articles about trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

trifluoro-methanesulfonic acid 4-[(acetyl-hydrazono)-(4-chloro-phenyl)-methyl]-phenyl ester (128914-68-1) → trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester (220910-81-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1002/1526-4998(200102)57:2<191::AID-PS275>3.0.CO;2-O

Reference yield:

4-(4-chlorobenzoyl)phenyl trifluoromethanesulfonate → trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester (220910-81-6)

Guidance literature:

Multi-step reaction with 3 steps

1: NH₂NH₂; AcOH / ethanol / Heating

2: Et₃N / 0 - 20 °C

3: 41 percent / H₂ / Pd/C / ethyl acetate

With hydrogen; acetic acid; triethylamine; hydrazine; palladium on activated charcoal; In ethanol; ethyl acetate;

DOI:10.1002/1526-4998(200102)57:2<191::AID-PS275>3.0.CO;2-O

Reference yield:

trifluoro-methanesulfonic acid 4-[(4-chloro-phenyl)-hydrazono-methyl]-phenyl ester (83887-80-3) → trifluoro-methanesulfonic acid 4-[(N'-acetyl-hydrazino)-(4-chloro-phenyl)-methyl]-phenyl ester (220910-81-6)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / 0 - 20 °C

2: 41 percent / H₂ / Pd/C / ethyl acetate

With hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate;

DOI:10.1002/1526-4998(200102)57:2<191::AID-PS275>3.0.CO;2-O

upstream raw materials:

trifluoro-methanesulfonic acid 4-[(acetyl-hydrazono)-(4-chloro-phenyl)-methyl]-phenyl ester

trifluoro-methanesulfonic acid 4-[(4-chloro-phenyl)-hydrazono-methyl]-phenyl ester

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