tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine

Base Information

Chemical Name:tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine
CAS No.:112306-72-6
Molecular Formula:C₄₇H₆₅N₉O₁₀
Molecular Weight:916.087
Hs Code.:

Synonyms:tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine

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Chemical Property of tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine

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Technology Process of tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine

There total 7 articles about tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13512-59-9
N-(tert-butyloxycarbonyl)-O-(phenylmethyl)-L-tyrosine 4-nitrophenol ester

: 112306-72-6
tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) H₂; 2) 1M aq. NaOH / Pd black / 1) methanol, 3 h; 2) DMF, 24 h, room temp.

2: 83 percent / N,N'-dicyclohexylcarbodiimide / dimethylformamide / 1) -25 deg C, 45 min.; 2) 24 h, room temp.

3: 1) H₂ / Pd black / 1) methanol, 3 h; 2) DMF, 24 h, room temp.

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; palladium; In N,N-dimethyl-formamide;

Reference yield:

: 34286-66-3
N-benzyloxycarbonyl-(R)alanyl-glycine

: 112306-72-6
tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) H₂; 2) 1M aq. NaOH / Pd black / 1) methanol, 3 h; 2) DMF, 24 h, room temp.

2: 83 percent / N,N'-dicyclohexylcarbodiimide / dimethylformamide / 1) -25 deg C, 45 min.; 2) 24 h, room temp.

3: 1) H₂ / Pd black / 1) methanol, 3 h; 2) DMF, 24 h, room temp.

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; palladium; In N,N-dimethyl-formamide;

Reference yield:

: 67706-16-5
tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycine

: 112306-72-6
tert-butyloxycarbonyl-O-benzyl-L-tyrosyl-D-alanyl-glycyl-L-phenylalanyl-L-tert-leucyl-L-arginine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / N,N'-dicyclohexylcarbodiimide / dimethylformamide / 1) -25 deg C, 45 min.; 2) 24 h, room temp.

2: 1) H₂ / Pd black / 1) methanol, 3 h; 2) DMF, 24 h, room temp.

With hydrogen; dicyclohexyl-carbodiimide; palladium; In N,N-dimethyl-formamide;