4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile

Base Information

Chemical Name:4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile
CAS No.:334912-42-4
Molecular Formula:C₄₂H₇₂N₂O₁₀
Molecular Weight:765.041
Hs Code.:

Synonyms:4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile

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Chemical Property of 4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile

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Technology Process of 4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile

There total 6 articles about 4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 334912-41-3
1,2-dibromo-4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-benzene

: 334912-42-4
4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile

Guidance literature:: In N,N-dimethyl-formamide; for 6h; Heating;
DOI:10.1021/ja004034i

Reference yield:

: 334912-39-9
10-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}decan-1-ol

: 334912-42-4
4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 111.06 g / NaOH / H₂O; tetrahydrofuran / 6 h / 0 - 20 °C

2: 57 percent / LiBr*H₂O / acetone / 3 h / Heating

3: 67 percent / K₂CO₃ / acetonitrile / 48 h / Heating

4: 82 percent / dimethylformamide / 6 h / Heating

With sodium hydroxide; potassium carbonate; lithium bromide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja004034i

Reference yield:

: toluene-4-sulfonic acid 10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyl ester

: 334912-42-4
4,5-bis-(10-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-decyloxy)-phthalonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / LiBr*H₂O / acetone / 3 h / Heating

2: 67 percent / K₂CO₃ / acetonitrile / 48 h / Heating

3: 82 percent / dimethylformamide / 6 h / Heating

With potassium carbonate; lithium bromide; In N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja004034i