Technology Process of C25H36FN5O4Si
There total 6 articles about C25H36FN5O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonia;
In
methanesulfonic acid;
at 100 ℃;
for 5h;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic acid; water / tetrahydrofuran / 3 h / 0 °C
2: Dess-Martin periodane / dichloromethane / 1 h / Inert atmosphere
3: tetrahydrofuran; diethyl ether / 5 h / -78 - 0.1 °C
4: ammonia / methanesulfonic acid / 5 h / 100 °C / Sealed tube
With
ammonia; water; Dess-Martin periodane; trifluoroacetic acid;
In
tetrahydrofuran; methanesulfonic acid; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Dess-Martin periodane / dichloromethane / 1 h / Inert atmosphere
2: tetrahydrofuran; diethyl ether / 5 h / -78 - 0.1 °C
3: ammonia / methanesulfonic acid / 5 h / 100 °C / Sealed tube
With
ammonia; Dess-Martin periodane;
In
tetrahydrofuran; methanesulfonic acid; diethyl ether; dichloromethane;