meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin

Base Information

• Chemical Name: meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin
• CAS No.: 1438391-21-9
• Molecular Formula: C₄₇H₃₇N₅O₅
• Molecular Weight: 751.841

Synonyms:meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin

Chemical Property of meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin

Chemical Property:

Purity/Quality:

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Technology Process of meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin

There total 2 articles about meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

meso-tetrakis(4-methoxyphenyl)-2-(N-amino-aza)-3-oxoporphyrin → meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin (1438391-21-9)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; 1,2-dichloro-benzene; for 14h; Reflux;

DOI:10.1039/c3ob40138c

Reference yield:

meso-tetrakis(4-methoxyphenyl)-2-oxa-3-oxoporphyrin → meso-tetrakis(4-methoxyphenyl)-2-aza-3-oxoporphyrin (1438391-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate monohydrate / tetrahydrofuran / 120 h / Reflux

2: samarium diiodide / tetrahydrofuran; 1,2-dichloro-benzene / 14 h / Reflux

With samarium diiodide; hydrazine hydrate monohydrate; In tetrahydrofuran; 1,2-dichloro-benzene;

DOI:10.1039/c3ob40138c

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