ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside

Base Information

Chemical Name:ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside
CAS No.:1312541-38-0
Molecular Formula:C₁₈H₂₀Cl₂O₇S
Molecular Weight:451.325
Hs Code.:

Synonyms:ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside

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Chemical Property of ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside

Chemical Property:

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Technology Process of ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside

There total 1 articles about ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1263058-23-6
ethyl 2-O-benzoyl-3-O-chloroacetyl-1-thio-α-D-arabinofuranoside

: 541-88-8
Chloroacetic anhydride

: 1312541-38-0
ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1055/s-0031-1290752

Reference yield: 76.0%

: 1263058-13-4
2-chloroethyl 2,3-di-O-benzoyl-α-D-arabinofuranoside

: 1312541-38-0
ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside

: 1312541-24-4
C₃₇H₃₅Cl₃O₁₄

Guidance literature:: With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; at -20 ℃; Molecular sieve;
DOI:10.1007/s11172-010-0397-4

Reference yield:

: 1312541-38-0
ethyl 2-O-benzoyl-3,5-bis-O-(chloroacetyl)-1-thio-α-D-arabinofuranoside

: 1289100-85-1
C₃₃H₃₃ClO₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate / dichloromethane / -20 °C / Molecular sieve

2: pyridine; water / 2 h / 70 °C

With pyridine; N-iodo-succinimide; water; triethylsilyl trifluoromethyl sulfonate; In dichloromethane;
DOI:10.1007/s11172-010-0397-4