Technology Process of C25H28O5S
There total 7 articles about C25H28O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; palladium diacetate; caesium carbonate;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 8h;
DOI:10.1016/j.tet.2013.04.090
- Guidance literature:
-
Multi-step reaction with 4 steps
1: p-toluenesulfonyl chloride; pyridine
2: triethylamine / chloroform / 3 h / 20 °C
3: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0 - 20 °C
4: palladium diacetate; caesium carbonate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 8 h / 100 °C
With
pyridine; tetrabutylammomium bromide; palladium diacetate; caesium carbonate; triethylamine; p-toluenesulfonyl chloride; sodium hydroxide;
In
dichloromethane; chloroform; water; N,N-dimethyl-formamide;
4: |Heck Reaction;
DOI:10.1016/j.tet.2013.04.090
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / chloroform / 3 h / 20 °C
2: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0 - 20 °C
3: palladium diacetate; caesium carbonate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 8 h / 100 °C
With
tetrabutylammomium bromide; palladium diacetate; caesium carbonate; triethylamine; sodium hydroxide;
In
dichloromethane; chloroform; water; N,N-dimethyl-formamide;
3: |Heck Reaction;
DOI:10.1016/j.tet.2013.04.090
